Coulometric KF Titrator MKC-710S

Coulometric Karl Fischer Titrator MKC-710S
Coulometric Karl Fischer Titrator MKC-710S
Coulometric Karl Fischer Titrator MKC-710S with IDP-100 printer

Large user touch panel - convenient operation: The MKC-710S titrator comes with a large TFT colour touch screen. The MKC-710S is ideally suited to measure samples which only release their water slowly or at elevated temperatures: It can remote control the ADP-611 evaporator and visualize the evaporation curve on the display and printout.

Fast measurements
A new acceleration amplifier provides faster electrolysis with a maximum electrolytic speed of 2.6 mg H2O/min. This shortens the time required for pre-titrations and sample measurements considerably.

Paper saving
Paper saving and environmentally friendly – results no longer need to be printed: Measurement results are converted to PDF and can be stored in a USB flash drive.

Details

User groups and permissions

Two different user levels let you easily define the operation permissions of each operator. An administrator (protected with password) has access to all functions whereas a normal operator can only perform burette operation, calibration, measurement, method number (sample file) change and reading of method.

The AT-710 Titrator is compatible with a wide range of USB devices
Two different user levels let you easily define the operation permissions of each operator.
Two different user levels let you easily define the operation permissions of each operator.

Easy cleaning and maintenance

The MKC-710S coulometric Karl Fischer Titrator can be equipped with a titration cell with a replaceable ceramic diaphragm. It is thus the ideal solution to measure dirty and sticky samples with a low water content as eg. oils.

The MKC-710 Coluometric Karl Fischer Titrators can be equipped with a coulometric cell with a removable diaphragm.
The MKC-710 coulometric Karl Fischer Titrators can be equipped with a titration cell with a replaceable ceramic diaphragm.

Ideally suited for the heating method

The MKC-710S is ideally suited to measure samples which only release their water slowly or at elevated temperatures: It can remote control the ADP-611 evaporator and visualize the evaporation curve on the display and printout. This allows to define all the measuring parameters including the purge cycles and the temperature in the evaporator in one single method and simplifies method development.

The MKC-710 colulometric Karl Fischer Titrators  can remote control the ADP-611 evaporator and visualize the evaporation curve on the display and printout.
The MKC-710 Titrators can remote control the ADP-611 evaporator and visualize the evaporation curve on the display and printout.
ADP-611 evaporator

Smooth data entry and control

Transmitting sample weights directly from a balance, inputting sample names with a barcode reader, entering sample codes with a numeric keypad: The MKC-710S titrator offers all the interfaces and features required for a seamless integration into your workflow.

The AT-710 Titrator is compatible with a wide range of USB devices
The AT-710 and MKV/MKC-710 titrators are compatible with a wide range of USB devices.

Applications

Food and Beverage

  • Cooking fat
  • Olive oil
  • Peanut oil
  • Rapeseed oil
  • Safflower oil
  • Soy bean oil

Chemicals / Petrochemicals

  • ABS (9)
  • Acenaphthene
  • Aerosil (13)
  • Aldehydes (2)
  • Alizarin
  • Allocymol
  • Allyl chloride
  • Amyl acetate
  • Anisole
  • Aviation gasoline (5) (6)
  • Benzene (1)
  • Benzil
  • Benzoin
  • Benzophenone
  • Benzyl alcohol
  • Benzyl bromide
  • Benzyl chloride
  • Benzyl phenyl ketone
  • Biodiesel
  • Biphenyl
  • Bromodecane
  • Bromoform
  • Bromohexadecane
  • Bromoisobutyric acid ester
  • Bromotetradecane
  • Butane (25)
  • Butane (25)
  • Butanol
  • Butyl acetate
  • Camphor
  • Caprolactam (10)
  • Carbazinic acid methyl ester
  • Carbon black (18)
  • Carbon dioxide (25)
  • Carbon powder (18)
  • Carbon tetrachloride
  • Cetyl alcohol
  • Chloral
  • Chlorobenzene
  • Chloroform
  • Chlorooctane
  • Chlorophenol
  • Chlorotoluene
  • Coal powder and dust (18)
  • Cresol
  • Crude oil (4)
  • Cyclododecane
  • Cycloheptane
  • Cyclohexane
  • Cyclohexanol
  • Cyclohexyl chloride
  • Decylcyclohexane
  • Dibenzylideneacetone
  • Dibromomethane
  • Dichlorobenzene
  • Dichloroethane
  • Dichloromethane
  • Dichlorophenol
  • Dichlorotetrafluoroacetone
  • Dicyclopentadiene
  • Didecyl ether
  • Diesel fuel (5) (6)
  • Diethyl ether
  • Diethyleneglycol diethyl ether
  • Diethyleneglycol monomethyl ether
  • Difluorobenzene
  • Diheptyl ether
  • Diisopropyl ketone
  • Dimethyl terephthalate
  • Dimethylbutane
  • Dimethylnaphthalene
  • Dimethylpentanol
  • Dimethylstyrene
  • Dioxane
  • Dodecane (1)
  • Dodecanol
  • Epoxy resin (11)
  • Ethanol (4)
  • Ether
  • Ethyl acetate
  • Ethyl acetoacetate
  • Ethyl acrylate
  • Ethyl Laevulinate
  • Ethyl propionate
  • Ethylene glycol
  • Ethylene oxide (25)
  • Ethylhexanol
  • Ethylhexyl nitrate
  • Ethyltoluene
  • Fluorene
  • Fluoroanisole
  • Fluorophenol
  • Formaldehyde
  • Freons (25)
  • Gasoline (5) (6)
  • Geraniol
  • Glass fibers and powder (24)
  • Glycerol
  • Glycerol monostearate
  • Grease (7)
  • Guaethol
  • Gypsum (13)
  • Heptanol
  • Hexane
  • Hexanetriol
  • Hexanol
  • Hexylene glycol
  • Hydraulic oil (3)
  • Hydrocarbons (1)
  • Icosane
  • Insulating oil (3)
  • Iodoanisole
  • Iodoethane
  • Iodomethane
  • Iodonaphthene
  • Isopropanol
  • Kerosene (5) (6)
  • Ketones (2)
  • Lubricating oil (7)
  • Mannitol
  • Melamine resin (9)
  • Methane (25)
  • Methanol
  • Methoxybenzene
  • Methyl salicylate
  • Methylbutadiene
  • Methylcyclohexane
  • Methylenephenanthrene
  • Methylpentanediol
  • Methylpentanol
  • Motor oil (7)
  • Natural gas (25)
  • Nitrogen (25)
  • Nitrophenol
  • Nonanol
  • Norbornadiene
  • Nylon 6 / Nylon 66 (12)
  • Octacosane
  • Octane
  • Octanol
  • Oxygen (25)
  • Pentane
  • Pentanediol
  • Petroleum
  • Phenol
  • Phenol-formaldehyde resins (13)
  • Phenoxyethanol
  • Phenylpropanol
  • Plastics (8)
  • Polyacrylamide (13)
  • Polyamide (12)
  • Polycarbodiimide (14)
  • Polycarbonate (15)
  • Polyester (16)
  • Polyether (14)
  • Polyethylene (13)
  • Polyethylene glycol
  • Polyethylene terephthalate (17)
  • Polyimide (9)
  • Polyisobutylene (18)
  • Polymethylmethacrylate (19)
  • Polyoxymethylene (9)
  • Polypropylene (20)
  • Polystyrene (11)
  • Polyurethane (19)
  • Polyvinyl acetate (21)
  • Polyvinyl butyral (PVB) (14)
  • Propane (25)
  • Propane (25)
  • Propanol
  • Propylene oxide (25)
  • Propylene oxide (25)
  • PTFE (22)
  • Rubber (22)
  • Silicone oil (26)
  • Silicone rubber (22)
  • Soft PVC (15)
  • Sorbitol
  • Stearyl alcohol
  • Styrene acrylate (21)
  • Sulfur dioxide (25)
  • Teflon (22)
  • Terephthalic acid esters (14)
  • Tetrabromoethane
  • Tetrachloroethane
  • Tetradecene (1)
  • Transformer oil (3)
  • Trichloroethane
  • Trimethylstyrene
  • Trioxane
  • Turbine oil (3)
  • Urea-formaldehyde resin
  • Vinyl chloride (25)
  • Vinylcyclohexane
  • Xylene

Standards

ASTMD 1533-00
ASTMD 3401-97
ASTM D 4928-11
ASTM E 1064-08

DIN 51777
EN ISO 12937:2002-03

ISO 10337
ISO 10338
ISO 10339
ISO 10340
ISO 10341
ISO 10342

Remarks (1) ... (26)

Pharmaceuticals, Flavours & Fragrances, Cosmetics

  • Baby oils
  • Almond oils
  • Didecyl ether
  • Resorcinol dimethyl ether
  • Serotonin (13)

Standards

ASTM D 4928-11

Remarks (1) ... (26)

Technical Specifications

Type and model name

MKC-710S Coulometric Karl Fischer Moisture Titrator

 

Product configuration

MCU-710S + MKC-710, IDP-100 Printer, Manual Solvent Change Unit

Titration Methods

120 freely assignable methods

Karl Fischer Coulometric Titration
Bromine Index 

 
Measuring range Water content / Bromine Index 10 μg … 300 mg (depending on reagent)
Precision Relative standard deviation
(Based on KEM's standard measuring conditions and standard liquids) 
< 0.3% (n=10)
Display Resolution 0.1 μg  

Generator electrode

With or without diaphragm

 

Control method

Constant current pulse time control

 
Endpoint detection Polarized twin Pt electrode (AC)  
Endpoint sense

EP is detected when the drift is getting stable or when a preset limit time for the titration has been reached,

Solvent quantity required Anolyte
Catholyte 
100 mL (max. 150 mL)
5mL 
Display

8.4 inch color LCD 800 x 600 dots touch screen

User interface

1-channel display

Languages: Japanese / English / Mandarin Chinese / Korean / Russian / Spanish / German / French

Calculations Water content, statistics (mean, SD and RSD) and automatic averaging of blank values  
Data storage On board memory:  500 results
GLP functions

Operators:

 
Reagents:

Performance checks:

 

Up to 10 operators can be registered.
User group administration.

Alert when Anolyte or Catholyte needs to be replaced

Reminder of scheduled check date, record of check results.

Operating hours counter.


 

External I/O

RS-232C, 4 channels

 
USB, 1 port 

for dot matrix printer, electronic balance, evaporator, Data Capture Software (SOFT-CAP)

for USB flash drive, thermal printer, keyboard, barcode reader, foot switch, USB hub

Extensibility

Evaporator  ADP-611

 
Ambient conditions Temperature:
Rel. humidity:
 5 … 35 °C
 < 85% (no condensation)
Power supply AC 100 … 240 V ±10 % 50/60 Hz (comes with AC adapter)  
Power consumption Main unit
Printer 
approx. 30W
approx. 7W 
Dimensions Touch panel controller
Titration unit:
Stirrer:
Solvent Change Unit:
Printer: 
225(W) × 190(D) × 42(H) mm
141(W) × 292(D) × 244(H) mm
107(W) × 206(D) × 340(H) mm (without Solvent Change Unit)
240(W) × 140(D) × 405(H) mm (without tubing)
106(W) × 180(D) × 88(H) mm 
Weight Touch panel controller
Titration unit:
Stirrer:
Solvent Change Unit:
Printer: 
approx. 1.5 kg
approx. 3.0 kg
approx. 2.0 kg
approx. 0.6 kg
approx. 0.4 kg 
Conformity standard CE marking EMC : EN61326-1 LVD: EN61010-1  

Software

Soft Cap Data Capture Software

SOFT CAP Data Capture Software
SOFT CAP Data Capture Software

The easy way to transfer your results directly to Microsoft EXCEL

The Data Capture Software is an easy to use and flexible solution to collect measurement results from different KEM instruments (Refractometers, Density Meters, Potentiometric or Karl-Fischer Titrators, Thermal Conductivity Meters) on a Windows personal computer.

  • Up to four different instruments can be connected to one single PC and be used simultaneously. Two of these instruments can be of the same model.
  • The results can directly be stored in EXCEL workbooks. The measured results are always available at a glance in a clear and concise manner.
    • As soon as a measurement has finished, the result appears in the corresponding worksheet.
    • The layout, order and the format how the results are stored in EXCEL can freely be adapted to specific needs.
    • Results can be automatically be processed by EXCEL macros as they are transmitted to the PC. Additional data (comments, sample data, etc.) can be entered at any time by means of the PC keyboard or a barcode reader.
  • All results can at the same time be stored in as CSV files.

System Requirements for PC

SpecificationDescription
Computer Personal computer with Pentium II CPU of 233MHz or better
Operating system Microsoft Windows 2000, XP,
Vista (Home Basic, Business), 7 (Home Premium, Professional)
Other programs Microsoft EXCEL 97 / 2000 / 2003 / 2007
RAM at least 128 MB / 512 MB recommended
Hard disc space 10 MB required for installation
Display Resolution higher than 640 * 480
Disk drive CD-ROM or DVD-ROM
Interface 1 USB port
RS-232C D-sub (male) 9 pin required for each additional instrument
to be connected to the same computer.

Accessories

Printer

IDP-100 Printer
IDP-100 Printer

IDP-100 Printer

Dot matrix ink printer for GLP compliance.

  • Dot matrix printer with ink ribbon, prints on regular paper (width 57.5 ± 0.5mm).
  • 24 digits, 144 dots per line.
  • Automatic paper end detection - no loss of data!
  • 2 kB internal buffer memory. Advantage: Less time required per measurement, as the instrument does not have to wait until the results are printed out.

Evaporator

ADP-611 Evaporator
ADP-611 evaporator

ADP-611: Accurate water determinations of difficult samples

The ADP-611 substantially broadens the application spectrum of your Karl Fischer Titrator. With this evaporator accurate water determinations of samples which cannot be titrated directly can be performed:

  • Substances which cause side reactions with the KF reagent such as copper (II) salts, iron (III) salts, nitrites, motor oils with additives, etc.
  • Substances that release water only at elevated temperatures like plastics
  • Substances which would contaminate the titration cell like coal dust, carbon black, etc.
  • Substances that are poorly soluble or insoluble such as cotton, paper, compressed wood, etc.

The ADP-611 features a modern microprocessor control ensuring maximum precision, reliability and user-friendliness: 

  • Easy method development: A patented scan mode automatically determines the optimal evaporation temperature based on the relation between released water and heating temperature.
  • Rapid rise and accurate control of the heating temperature.
  • Digital display of temperature and flow rate.
  • Automatic alarm if the set temperature cannot be reached within a certain time or if the temperature in the oven exceeds 350°C.
  • Serial interface which enables the evaporator to be remote controlled by the MKA-610 and MKC-610 Karl Fischer titrators.

To safely avoid contamination from atmospheric moisture the ADP-611 is equipped with a remote controlled motor driven magnetic bar to move the sample from the sample chamber into the oven.

The heating chamber is equipped with an electrically conductive transparent heater glass. This permits the sample condition to be monitored during the vaporization process.

The ADP-611 comes with two built-in desiccant tubes for the carrier gas. With an optional air pump, air instead of nitrogen can be used as carrier gas.

 

Technical Specifications ADP-611
Heating system Electrically conductive transparent heating glass  
Temperature control Control method
Setting range
Temperature sensor
Temperature measurement precision
proportional
50 … 300 °C
K-thermocouple
± 2 °C
Display Temperature or flow, LED, 3 digits  
Heating tube Pyrex® glass tube 30 (ø) x 335 (L) mm
Sample boat Pyrex® glass
Capacity
68 (L) x 25 (W) x 15 (H) mm
16 mL
Carrier gas Nitrogen (not included in supplied parts)
Air (air pump optional)
Gas flow rate


100 … 300 mL/min
Gas dryer Zeolite 100 g 2 pcs (500 g Zeolite included in supplied parts)  
Interface RS-232 9 pin male for communication with KF titrator  
Ambient conditions Temperature: 5 … 35°C
Humidity: < 85% RH
 
Power Supply (set in factory)
Consumption
100 … 120 V, 200 … 240 V AC, 50/60 Hz
300 W
Dimensions 370 (W) x 195 (D) x 217 (H) mm  
Weight 100 … 120 V version
200 … 240 V version
approx. 5 kg
approx. 7 kg

Solvent Pump

Automatic pump to fill and empty the Karl Fischer titration cell
Automatic pump to fill and empty the Karl Fischer titration cell

Automatic filling and emptying system for titration cell

Direct contact with Karl Fischer Reagents should always be avoided. This automatic filling an emptying system for the titration cell (ordering number 98-433-0135) protects operators from direct contact with toxic reagents and vapors. The pump is built into the magnetic stirrer. The connecting cable for the stirrer is included in the standard delivery.

Titration Cells

SketchPart CodeDescription
coulometric_karl_fischer_cell_4200.png 20-040-4200-48 Transparent cell with drain cock (glass cell only)
coulometric_karl_fischer_cell_7300.png 12-006-7300-48 Transparent cell, complete, including generator electrode without diaphragm, twin Pt electrode, washing bottle, funnel, KF grease, septum (10 pcs.) and anode  adjuster
coulometric_karl_fischer_cell_7400.png 12-006-7400-48 Transparent cell, complete, including generator electrode with diaphragm, twin Pt electrode, washing bottle, funnel, KF grease, septum (10 pcs.) and anode  adjuster
coulometric_karl_fischer_cell_6200.png 12-006-6200-48 Transparent cell, including generator electrode without diaphragm and twin Pt electrode
coulometric_karl_fischer_cell_6100.png 12-006-6100-48 Transparent cell, including generator electrode with diaphragm and twin Pt electrode
coulometric_karl_fischer_cell_6300.png 12-006-6300-48 Transparent cell with drain cock, including generator electrode without diaphragm and twin Pt electrode
coulometric_karl_fischer_cell_6400.png 12-006-6400-48 Transparent cell with drain cock, including generator electrode with diaphragm and twin Pt electrode

Samplers

SketchPart CodeDescription
karl_fischer_sampler_3011.png 98-740-3011 Bent-type sampler for powders (1 … 1.5 mL)
karl_fischer_sampler_3020.png 98-740-3020 "C" bent-type sampler for powders
karl_fischer_sampler_3025.png 98-740-3025 Light weight sampler for powders
karl_fischer_sampler_3026.png 98-740-3026 Straight type light weight sampler
karl_fischer_sampler_3030.png 98-740-3030 Sampler for viscous products
karl_fischer_sampler_3031.png 98-740-3031 Sampler for highly viscous products
karl_fischer_sampler_4013.png 98-433-4013 Liquefied gas sampler with pressure vessel made of stainless steel (100 mL)
karl_fischer_sampler_3013.png 98-740-3013 Sampler for oils
karl_fischer_sampler_3012.png 98-740-3012 Spoon type sampler for viscous products
karl_fischer_sampler_3024.png 98-740-3024 Eggplant type sampler for powders
karl_fischer_sampler_3166.png 98-500-3166
98-500-3225
Syringe (5 mL)
Syringe (20 mL)
karl_fischer_sampler_3407.png 98-433-3407 Stopper for syringe inlet port
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