MKC-710 Titrator

Coulometric KF Titrator MKC-710S

Large user touch panel – convenient operation: The MKC-710S titrator comes with a large TFT colour touch screen. The MKC-710S is ideally suited to measure samples which only release their water slowly or at elevated

Product Description

Large user touch panel – convenient operation: The MKC-710S titrator comes with a large TFT colour touch screen. The MKC-710S is ideally suited to measure samples which only release their water slowly or at elevated temperatures: It can remote control the ADP-611 evaporator and visualize the evaporation curve on the display and printout.

Fast measurements
A new acceleration amplifier provides faster electrolysis with a maximum electrolytic speed of 2.6 mg H2O/min. This shortens the time required for pre-titrations and sample measurements considerably.

Paper saving
Paper saving and environmentally friendly – results no longer need to be printed: Measurement results are converted to PDF and can be stored in a USB flash drive.

Details

Applications

Technical Specifications

Software

Soft Cap Data Capture Software

SOFT CAP Data Capture Software

The easy way to transfer your results directly to Microsoft EXCEL

The Data Capture Software is an easy to use and flexible solution to collect measurement results from different KEM instruments (Refractometers, Density Meters, Potentiometric or Karl-Fischer Titrators, Thermal Conductivity Meters) on a Windows personal computer.

  • Up to four different instruments can be connected to one single PC and be used simultaneously. Two of these instruments can be of the same model.
  • The results can directly be stored in EXCEL workbooks. The measured results are always available at a glance in a clear and concise manner.
    • As soon as a measurement has finished, the result appears in the corresponding worksheet.
    • The layout, order and the format how the results are stored in EXCEL can freely be adapted to specific needs.
    • Results can be automatically be processed by EXCEL macros as they are transmitted to the PC. Additional data (comments, sample data, etc.) can be entered at any time by means of the PC keyboard or a barcode reader.
  • All results can at the same time be stored in as CSV files.

System Requirements for PC

Specification Description
Computer Personal computer with Pentium II CPU of 233MHz or better
Operating system Microsoft Windows 2000, XP,
Vista (Home Basic, Business), 7 (Home Premium, Professional)
Other programs Microsoft EXCEL 97 / 2000 / 2003 / 2007
RAM at least 128 MB / 512 MB recommended
Hard disc space 10 MB required for installation
Display Resolution higher than 640 * 480
Disk drive CD-ROM or DVD-ROM
Interface 1 USB port
RS-232C D-sub (male) 9 pin required for each additional instrument
to be connected to the same computer.

Accessories

Printer

IDP-100 Printer

IDP-100 Printer

Dot matrix ink printer for GLP compliance.

  • Dot matrix printer with ink ribbon, prints on regular paper (width 57.5 ± 0.5mm).
  • 24 digits, 144 dots per line.
  • Automatic paper end detection – no loss of data!
  • 2 kB internal buffer memory. Advantage: Less time required per measurement, as the instrument does not have to wait until the results are printed out.

Evaporator

ADP-611 Evaporator

ADP-611: Accurate water determinations of difficult samples

The ADP-611 substantially broadens the application spectrum of your Karl Fischer Titrator. With this evaporator accurate water determinations of samples which cannot be titrated directly can be performed:

  • Substances which cause side reactions with the KF reagent such as copper (II) salts, iron (III) salts, nitrites, motor oils with additives, etc.
  • Substances that release water only at elevated temperatures like plastics
  • Substances which would contaminate the titration cell like coal dust, carbon black, etc.
  • Substances that are poorly soluble or insoluble such as cotton, paper, compressed wood, etc.

The ADP-611 features a modern microprocessor control ensuring maximum precision, reliability and user-friendliness:

  • Easy method development: A patented scan mode automatically determines the optimal evaporation temperature based on the relation between released water and heating temperature.
  • Rapid rise and accurate control of the heating temperature.
  • Digital display of temperature and flow rate.
  • Automatic alarm if the set temperature cannot be reached within a certain time or if the temperature in the oven exceeds 350°C.
  • Serial interface which enables the evaporator to be remote controlled by the MKA-610 and MKC-610 Karl Fischer titrators.

To safely avoid contamination from atmospheric moisture the ADP-611 is equipped with a remote controlled motor driven magnetic bar to move the sample from the sample chamber into the oven.

The heating chamber is equipped with an electrically conductive transparent heater glass. This permits the sample condition to be monitored during the vaporization process.

The ADP-611 comes with two built-in desiccant tubes for the carrier gas. With an optional air pump, air instead of nitrogen can be used as carrier gas.

 

Technical Specifications ADP-611
Heating system Electrically conductive transparent heating glass
Temperature control Control method
Setting range
Temperature sensor
Temperature measurement precision
proportional
50 … 300 °C
K-thermocouple
± 2 °C
Display Temperature or flow, LED, 3 digits
Heating tube Pyrex® glass tube 30 (ø) x 335 (L) mm
Sample boat Pyrex® glass
Capacity
68 (L) x 25 (W) x 15 (H) mm
16 mL
Carrier gas Nitrogen (not included in supplied parts)
Air (air pump optional)
Gas flow rate
100 … 300 mL/min
Gas dryer Zeolite 100 g 2 pcs (500 g Zeolite included in supplied parts)
Interface RS-232 9 pin male for communication with KF titrator
Ambient conditions Temperature: 5 … 35°C
Humidity: < 85% RH
Power Supply (set in factory)
Consumption
100 … 120 V, 200 … 240 V AC, 50/60 Hz
300 W
Dimensions 370 (W) x 195 (D) x 217 (H) mm
Weight 100 … 120 V version
200 … 240 V version
approx. 5 kg
approx. 7 kg

Solvent Pump

Automatic pump to fill and empty the Karl Fischer titration cell

Automatic filling and emptying system for titration cell

Direct contact with Karl Fischer Reagents should always be avoided. This automatic filling an emptying system for the titration cell (ordering number 98-433-0135) protects operators from direct contact with toxic reagents and vapors. The pump is built into the magnetic stirrer. The connecting cable for the stirrer is included in the standard delivery.

Titration Cells

Sketch Part Code Description
20-040-4200-48 Transparent cell with drain cock (glass cell only)
12-006-7300-48 Transparent cell, complete, including generator electrode without diaphragm, twin Pt electrode, washing bottle, funnel, KF grease, septum (10 pcs.) and anode  adjuster
12-006-7400-48 Transparent cell, complete, including generator electrode with diaphragm, twin Pt electrode, washing bottle, funnel, KF grease, septum (10 pcs.) and anode  adjuster
12-006-6200-48 Transparent cell, including generator electrode without diaphragm and twin Pt electrode
12-006-6100-48 Transparent cell, including generator electrode with diaphragm and twin Pt electrode
12-006-6300-48 Transparent cell with drain cock, including generator electrode without diaphragm and twin Pt electrode
12-006-6400-48 Transparent cell with drain cock, including generator electrode with diaphragm and twin Pt electrode

Samplers

Sketch Part Code Description
98-740-3011 Bent-type sampler for powders (1 … 1.5 mL)
98-740-3020 “C” bent-type sampler for powders
98-740-3025 Light weight sampler for powders
98-740-3026 Straight type light weight sampler
98-740-3030 Sampler for viscous products
98-740-3031 Sampler for highly viscous products
98-433-4013 Liquefied gas sampler with pressure vessel made of stainless steel (100 mL)
98-740-3013 Sampler for oils
98-740-3012 Spoon type sampler for viscous products
98-740-3024 Eggplant type sampler for powders
98-500-3166
98-500-3225
Syringe (5 mL)
Syringe (20 mL)
98-433-3407 Stopper for syringe inlet port
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Coulometric KF Titrator MKC-710S